Notebook
Prep - A laboratory notebook is required of
all Chemistry
121 students. Before coming to lab, students should prepare a
notebook write-up of the current experiment. Students are given
up to 10 points each week for their notebook prep. The notebook
prep should include:
- Purpose – What is the
purpose of doing this
experiment? What are we trying to learn / accomplish /
analyze? This section should answer these questions in a very
brief statement (two to three sentences is sufficient).
- Procedure – Exactly how
is this experiment carried
out? This section should precisely
outline the steps needed to
correctly perform this experiment. A rule of thumb is that you
should be able to do the experiment by only looking at your notebook
write-up.
- Data Table – This section
can take several
formats:
- The laboratory manual includes a report sheet for each
experiment. This is a useful guideline for your data section, and
could be written directly into your notebook.
- You could also
include blanks for your data throughout the procedure write-up.
For example, "Weigh the crucible and cover on the analytical
balance. Mass =
26.5022 g". Either method is
acceptable; use whichever feels better to you.
- Enough Space – Most
importantly, GIVE YOURSELF
ENOUGH SPACE! You do not have to fit everything on a single
page. You have lots of pages in your notebook – use them!
Recording Data
- Once in the lab, you will conduct the
experiment and
record your data. Accurate data collection is essential for
completing your experiment and writing a thorough report. The
following elements are important to keep in mind when recording data:
- Organization – Make sure
the data you are recording
goes in the correct blank space!
- Neatness – There's
nothing worse than not being
able to read your data. Actually, what's worse is if your TA
can't read your data! If numbers run into each other, print is
illegible, or data runs off the page, you'll have poor results and may
even need to start again.
- Mistakes – Everyone makes
mistakes. If you
make one, simply put a single line through the error (i.e. 1.015 g it should still
be legible) and write the
correction beside it. DO NOT scribble out the entire number; this
is not good lab practice.
- Significant Figures – If
a beaker weighs 52.0000 g
on the analytical balance, it is incorrect to write “52 g”; the
significant figures would be incorrect and could alter later
calculations.
- Units – Simply recording
150.35 for a mass is
incorrect. Is it in grams? milligrams? pounds? tons? You'll
need to know the correct units to complete an accurate calculation
later.
- Visual Observations –
It's not enough to just write
“White” for a color of a precipitate. What if you have 10 white
precipitates? How will you tell them apart later? Be sure
to record the color, consistency (gelatinous, flocculent, powdery,
crystalline),
relative amount, odor, if bubbles are formed, etc.
- Put it in the Notebook! –
Most important, do not
record data in anyplace other than your lab notebook. This data
must be collected by your TA and should be complete and accurate.
Notebook Exercise:
There are several “mock” notebooks
online that
you will analyze and grade or answer questions about, keeping the above
guidelines in mind. Turn in a “grading sheet” that you create on
a piece of paper to your TA in one week. It should include scores
for each notebook and brief comments for each (both positive feedback
and constructive criticism). The parameters for accessing the notebooks
and grading them are listed below.
Notebook Preps:
These have been prepared for an
experiment by five different students.
| Grading Scale: |
10 points
|
Perfect |
(all components included) |
|
8
points |
Good |
(all there, but not neat
or
spaced
well) |
|
6 points |
Average |
(need to expand on certain
sections) |
|
4 points |
Poor |
(missing one section) |
|
2
points |
Awful
|
(missing
more than one section) |
* there may be more than one page
Recorded Data:
Data collected during an
experiment
by five different students.
Answer the following questions
for each data set:
- What is the volume of NaOH required for Trial 2?
- What happens when Kool-Aid reacts with NaHCO3?
You can only answer the question based on that student's data sheet,
and only answer with the data they provide. (Answering with
assumed or made-up data would be academic misconduct!) If the
answer cannot be found on the student's data sheet or is illegible,
simply write “no data found” on your grading sheet. Although this
may happen if a student collects data in a poor manner, it should not
be a common occurrence.
Your Notebook:
Your first notebook prep
is due for
Experiment #2 at the start of lab next week. Follow the
above guidelines to ensure full points!